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MWCNTs of various sizes were used and three kinds of electroless plating baths were prepared to form the Ni-P alloy matrix with varying phosphorus contents. Heat- treatments of the composite films were also carried out. The microstructures of the composite films were examined by scanning electron microscopy and X-ray diffraction. Frictional properties of the composite films were investigated using a ball-on-plate method. Ni-P alloy/MWCNT composite films with different phosphorus contents, classified as high phosphorus (12-13 mass %), medium phosphorus (6-8 mass %), and low phosphorus (2-4 mass %) types, were fabricated using electroless deposition. The Ni-P alloy/MWCNT composite films showed lower friction coefficients compared to Ni-P alloy films with the same phosphorus content both before and after heat-treatment. 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MWCNTs of various sizes were used and three kinds of electroless plating baths were prepared to form the Ni-P alloy matrix with varying phosphorus contents. Heat- treatments of the composite films were also carried out. The microstructures of the composite films were examined by scanning electron microscopy and X-ray diffraction. Frictional properties of the composite films were investigated using a ball-on-plate method. Ni-P alloy/MWCNT composite films with different phosphorus contents, classified as high phosphorus (12-13 mass %), medium phosphorus (6-8 mass %), and low phosphorus (2-4 mass %) types, were fabricated using electroless deposition. The Ni-P alloy/MWCNT composite films showed lower friction coefficients compared to Ni-P alloy films with the same phosphorus content both before and after heat-treatment. The friction coefficients of the films were affected by the microstructure and size of the MWCNTs, the composition of the Ni-P alloy matrix, and the heat-treatment. (c) 2010 The Electrochemical Society. 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