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The storage modulus of PA9-T is retained at up to 60 degrees C with increasing humidity, then dropped with further increases in temperature past 70 degrees C. The decrease in mechanical properties at 70 degrees C due to moisture uptake is found to be substantially improved by annealing to develop molecular packing and/or crystallization. In contrast, the storage modulus of very highly crystallized (50% crystallinity) nylon 6 decreases markedly with humidity at low temperatures such as 20 degrees C. Thus, PA9-T retains its mechanical properties in humid atmospheres at much higher temperatures than nylon 6. The crystalline X-ray diffraction peaks for nylon 6 corresponding to (002) + (202) of the a form shift upon absorption of moisture, speculated to be due to the weakening of hydrogen bonds and the subsequent conformational disordering of the chains. Unlike nylon 6, the crystalline peaks of PA9-T do not shift due to moisture uptake. This is considered to be attributable to that the long aliphatic chain in PA9-T forms the large hydrophobic domain, rendering PA9-T less hygroscopic than nylon 6. Additionally, strong hydrogen bonds formed by terephthalamide residues together with a strong stacking force of phenylene groups may also repel water, preventing moisture bind with the amide groups of PA9-T crystals. 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  1. 080 繊維学部
  2. 0801 学術論文

Hydration in a new semiaromatic polyamide observed by humidity-controlled dynamic viscoelastometry and X-ray diffraction

http://hdl.handle.net/10091/1105
http://hdl.handle.net/10091/1105
a4943e79-7369-4487-a8ef-62310265e8d2
名前 / ファイル ライセンス アクション
Hydration Hydration in a New Semiaromatic Polyamide.pdf (551.2 kB)
Item type 学術雑誌論文 / Journal Article(1)
公開日 2008-07-17
タイトル
言語 en
タイトル Hydration in a new semiaromatic polyamide observed by humidity-controlled dynamic viscoelastometry and X-ray diffraction
言語
言語 eng
資源タイプ
資源 http://purl.org/coar/resource_type/c_6501
タイプ journal article
著者 Uddin, AJ

× Uddin, AJ

WEKO 41340

Uddin, AJ

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Gotoh, Y

× Gotoh, Y

WEKO 41341

Gotoh, Y

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Ohkoshi, Y

× Ohkoshi, Y

WEKO 41342

Ohkoshi, Y

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Nagura, M

× Nagura, M

WEKO 41343

Nagura, M

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Endo, R

× Endo, R

WEKO 41344

Endo, R

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Hara, T

× Hara, T

WEKO 41345

Hara, T

Search repository
信州大学研究者総覧へのリンク
氏名 Gotoh, Y
URL http://soar-rd.shinshu-u.ac.jp/profile/ja.uVDmjekV.html
信州大学研究者総覧へのリンク
氏名 Ohkoshi, Y
URL http://soar-rd.shinshu-u.ac.jp/profile/ja.jUkejekV.html
出版者
出版者 JOHN WILEY & SONS INC
引用
内容記述タイプ Other
内容記述 JOURNAL OF POLYMER SCIENCE PART B-POLYMER PHYSICS. 43(13): 1640-1648 (2005)
書誌情報 JOURNAL OF POLYMER SCIENCE PART B-POLYMER PHYSICS

巻 43, 号 13, p. 1640-1648, 発行日 2005-07-01
内容記述
内容記述タイプ Other
内容記述 This is a preprint of an article published in JOURNAL OF POLYMER SCIENCE PART B-POLYMER PHYSICS 2005; 43(13): 1640-1648
資源タイプ(コンテンツの種類)
内容記述タイプ Other
内容記述 Article
ISSN
収録物識別子タイプ ISSN
収録物識別子 0887-6266
書誌レコードID
収録物識別子タイプ NCID
収録物識別子 AA10689160
他の資源との関係:URI
識別子タイプ URI
関連識別子 http://www3.interscience.wiley.com/journal/117932503/grouphome/home.html
関連名称 http://www3.interscience.wiley.com/journal/117932503/grouphome/home.html
DOI
識別子タイプ DOI
関連識別子 https://doi.org/10.1002/polb.20446
関連名称 10.1002/polb.20446
出版タイプ
出版タイプ AM
出版タイプResource http://purl.org/coar/version/c_ab4af688f83e57aa
WoS
表示名 Web of Science
URL http://gateway.isiknowledge.com/gateway/Gateway.cgi?&GWVersion=2&SrcAuth=ShinshuUniv&SrcApp=ShinshuUniv&DestLinkType=FullRecord&DestApp=WOS&KeyUT=000230023200008
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