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Reduction of 3d transition metal cations (Cu2+ and Ni2+) in the interlayer regions of the cation exchanged alumina-pillared micas was attempted using ethylene glycol or diethylene glycol. The Cu2+-exchanged pillared mica led to the formation of a pillared mica composite containing interlayer zero-valence Cu-0 metal clusters along with Cu-0 metal fine particles on external surfaces of pillared mica flakes when refluxed in either ethylene glycol or diethylene glycol. Ni2+ cations in the interlayer region were also found to be reducible by refluxing in diethylene glycol. The zero-valence metal contained in the refluxed products occurs in three forms: M-0 clusters in the interlayer region, elongated fine particles sandwiched between silicate layers, and submicron spherical particles on external surfaces of mica crystals. The zero-valence metal/alumina-pillared mica composites thus obtained largely retained the micropore properties of the alumina-pillared micas. (c) 2007 Elsevier Ltd. 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Preparation of M-0 metal/alumina-pillared mica composites (M = Cu, Ni) by in situ reduction of interlayer M2+ ions of alumina-pillared fluorine micas
http://hdl.handle.net/10091/976
http://hdl.handle.net/10091/976804ea3f4-cc23-4e4e-812f-5ce0665bc648
名前 / ファイル | ライセンス | アクション |
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mica_composites.pdf (882.5 kB)
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Item type | 学術雑誌論文 / Journal Article(1) | |||||
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公開日 | 2008-02-06 | |||||
タイトル | ||||||
言語 | en | |||||
タイトル | Preparation of M-0 metal/alumina-pillared mica composites (M = Cu, Ni) by in situ reduction of interlayer M2+ ions of alumina-pillared fluorine micas | |||||
言語 | ||||||
言語 | eng | |||||
DOI | ||||||
識別子タイプ | DOI | |||||
関連識別子 | https://doi.org/10.1016/j.materresbull.2007.01.009 | |||||
関連名称 | 10.1016/j.materresbull.2007.01.009 | |||||
資源タイプ | ||||||
資源 | http://purl.org/coar/resource_type/c_6501 | |||||
タイプ | journal article | |||||
著者 |
Yamaguchi, T
× Yamaguchi, T× Taruta, S× Yamakami, T× Kitajima, K |
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信州大学研究者総覧へのリンク | ||||||
氏名 | Yamaguchi, T | |||||
URL | http://soar-rd.shinshu-u.ac.jp/profile/ja.WVnVbpkh.html | |||||
信州大学研究者総覧へのリンク | ||||||
氏名 | Taruta, S | |||||
URL | http://soar-rd.shinshu-u.ac.jp/profile/ja.OacaZVkh.html | |||||
出版者 | ||||||
出版者 | PERGAMON-ELSEVIER SCIENCE LTD | |||||
引用 | ||||||
内容記述タイプ | Other | |||||
内容記述 | MATERIALS RESEARCH BULLETIN. 42(12): 2143-2149 (2007) | |||||
書誌情報 |
en : MATERIALS RESEARCH BULLETIN 巻 42, 号 12, p. 2143-2149, 発行日 2007-12-04 |
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資源タイプ(コンテンツの種類) | ||||||
内容記述タイプ | Other | |||||
内容記述 | Article | |||||
ISSN | ||||||
収録物識別子タイプ | ISSN | |||||
収録物識別子 | 0025-5408 | |||||
書誌レコードID | ||||||
収録物識別子タイプ | NCID | |||||
収録物識別子 | AA1126842X | |||||
出版タイプ | ||||||
出版タイプ | AM | |||||
出版タイプResource | http://purl.org/coar/version/c_ab4af688f83e57aa | |||||
WoS | ||||||
表示名 | Web of Science | |||||
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