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In order to remove contamination and always keep the electrode surface in an active condition, we have developed laser ablation voltammetry (LAV) using ablation effect of a strong laser pulse. In this study, the IAV was further developed as laser pulse sampled DC voltarnmetry (LPSDCV) by adopting a current sampling technique of sampled DC voltammetry. The current is sampled at a certain time delayed from the laser pulse irradiation or the potential step, and the currents are recorded as a function of the potential to construct a voltammogram. LPSDCV was applied to the determination of glucose with a copper electrode. Under the optimal conditions for the time constant, the delay time and the pulse energy, a well-defined voltammogram with a limiting current was obtained. The limiting current was proportional to the glucose concentration from 0.2 to 10 mmol dm(-3) with a correlation coefficient of 0.999. Further, the determination of glucose in bovine serum containing a large amount of protein was attempted by the standard addition method. The relationship between the added quantity of glucose and the limiting current showed a straight line, even in the bovine serum, although the analytical value was ca. 2-times larger than the certified value. The reason is assumed to be due to the interference of ascorbic acid and protein contained in the bovine serum."}]}, "item_creator": {"attribute_name": "著者", "attribute_type": "creator", "attribute_value_mlt": [{"creatorNames": [{"creatorName": "Shinkai, M"}], "nameIdentifiers": [{"nameIdentifier": "36703", "nameIdentifierScheme": "WEKO"}]}, {"creatorNames": [{"creatorName": "Wakiura, S"}], "nameIdentifiers": [{"nameIdentifier": "36704", "nameIdentifierScheme": "WEKO"}]}, {"creatorNames": [{"creatorName": "Hinoue, T"}], "nameIdentifiers": [{"nameIdentifier": "36705", "nameIdentifierScheme": "WEKO"}]}]}, "item_files": {"attribute_name": "ファイル情報", "attribute_type": "file", "attribute_value_mlt": [{"accessrole": "open_date", "date": [{"dateType": "Available", "dateValue": "2015-09-28"}], "displaytype": "detail", "download_preview_message": "", "file_order": 0, "filename": "Bunseki_Kagaku.pdf", "filesize": [{"value": "359.6 kB"}], "format": "application/pdf", "future_date_message": "", "is_thumbnail": false, "licensetype": "license_note", "mimetype": "application/pdf", "size": 359600.0, "url": {"label": "Bunseki_Kagaku.pdf", "url": "https://soar-ir.repo.nii.ac.jp/record/11974/files/Bunseki_Kagaku.pdf"}, "version_id": "802e528b-aaaa-464f-9d3f-9c724d712e2d"}]}, "item_language": {"attribute_name": "言語", "attribute_value_mlt": [{"subitem_language": "eng"}]}, "item_resource_type": {"attribute_name": "資源タイプ", "attribute_value_mlt": [{"resourcetype": "journal article", "resourceuri": "http://purl.org/coar/resource_type/c_6501"}]}, "item_title": "Development of laser pulse sampled DC voltammetry and its application to the determination of glucose", "item_titles": {"attribute_name": "タイトル", "attribute_value_mlt": [{"subitem_title": "Development of laser pulse sampled DC voltammetry and its application to the determination of glucose", "subitem_title_language": "en"}]}, "item_type_id": "6", "owner": "1", "path": ["1170"], "permalink_uri": "http://hdl.handle.net/10091/1019", "pubdate": {"attribute_name": "PubDate", "attribute_value": "2008-03-31"}, "publish_date": "2008-03-31", "publish_status": "0", "recid": "11974", "relation": {}, "relation_version_is_last": true, "title": ["Development of laser pulse sampled DC voltammetry and its application to the determination of glucose"], "weko_shared_id": -1}
Development of laser pulse sampled DC voltammetry and its application to the determination of glucose
http://hdl.handle.net/10091/1019
http://hdl.handle.net/10091/10197919227c-6383-4759-8e78-fc5a851be895
名前 / ファイル | ライセンス | アクション |
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Item type | 学術雑誌論文 / Journal Article(1) | |||||
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公開日 | 2008-03-31 | |||||
タイトル | ||||||
言語 | en | |||||
タイトル | Development of laser pulse sampled DC voltammetry and its application to the determination of glucose | |||||
言語 | ||||||
言語 | eng | |||||
資源タイプ | ||||||
資源 | http://purl.org/coar/resource_type/c_6501 | |||||
タイプ | journal article | |||||
著者 |
Shinkai, M
× Shinkai, M× Wakiura, S× Hinoue, T |
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信州大学研究者総覧へのリンク | ||||||
氏名 | Hinoue, T | |||||
URL | http://soar-rd.shinshu-u.ac.jp/profile/ja.jmTajpnU.html | |||||
出版者 | ||||||
出版者 | JAPAN SOC ANALYTICAL CHEMISTRY | |||||
引用 | ||||||
内容記述タイプ | Other | |||||
内容記述 | BUNSEKI KAGAKU. 57(1): 61-65 (2008) | |||||
書誌情報 |
BUNSEKI KAGAKU 巻 57, 号 1, p. 61-65, 発行日 2008-01 |
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資源タイプ(コンテンツの種類) | ||||||
内容記述タイプ | Other | |||||
内容記述 | Article | |||||
ISSN | ||||||
収録物識別子タイプ | ISSN | |||||
収録物識別子 | 0525-1931 | |||||
書誌レコードID | ||||||
収録物識別子タイプ | NCID | |||||
収録物識別子 | AN00222633 | |||||
DOI | ||||||
識別子タイプ | DOI | |||||
関連識別子 | https://doi.org/10.2116/bunsekikagaku.57.61 | |||||
関連名称 | 10.2116/bunsekikagaku.57.61 | |||||
出版タイプ | ||||||
出版タイプ | AM | |||||
出版タイプResource | http://purl.org/coar/version/c_ab4af688f83e57aa | |||||
WoS | ||||||
表示名 | Web of Science | |||||
URL | http://gateway.isiknowledge.com/gateway/Gateway.cgi?&GWVersion=2&SrcAuth=ShinshuUniv&SrcApp=ShinshuUniv&DestLinkType=FullRecord&DestApp=WOS&KeyUT=000252607400009 |