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In order to remove contamination and always keep the electrode surface in an active condition, we have developed laser ablation voltammetry (LAV) using ablation effect of a strong laser pulse. In this study, the IAV was further developed as laser pulse sampled DC voltarnmetry (LPSDCV) by adopting a current sampling technique of sampled DC voltammetry. The current is sampled at a certain time delayed from the laser pulse irradiation or the potential step, and the currents are recorded as a function of the potential to construct a voltammogram. LPSDCV was applied to the determination of glucose with a copper electrode. Under the optimal conditions for the time constant, the delay time and the pulse energy, a well-defined voltammogram with a limiting current was obtained. The limiting current was proportional to the glucose concentration from 0.2 to 10 mmol dm(-3) with a correlation coefficient of 0.999. Further, the determination of glucose in bovine serum containing a large amount of protein was attempted by the standard addition method. The relationship between the added quantity of glucose and the limiting current showed a straight line, even in the bovine serum, although the analytical value was ca. 2-times larger than the certified value. 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  1. 040 理学部
  2. 0401 学術論文

Development of laser pulse sampled DC voltammetry and its application to the determination of glucose

http://hdl.handle.net/10091/1019
http://hdl.handle.net/10091/1019
7919227c-6383-4759-8e78-fc5a851be895
名前 / ファイル ライセンス アクション
Bunseki_Kagaku.pdf Bunseki_Kagaku.pdf (359.6 kB)
Item type 学術雑誌論文 / Journal Article(1)
公開日 2008-03-31
タイトル
言語 en
タイトル Development of laser pulse sampled DC voltammetry and its application to the determination of glucose
言語
言語 eng
資源タイプ
資源 http://purl.org/coar/resource_type/c_6501
タイプ journal article
著者 Shinkai, M

× Shinkai, M

WEKO 36703

Shinkai, M

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Wakiura, S

× Wakiura, S

WEKO 36704

Wakiura, S

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Hinoue, T

× Hinoue, T

WEKO 36705

Hinoue, T

Search repository
信州大学研究者総覧へのリンク
氏名 Hinoue, T
URL http://soar-rd.shinshu-u.ac.jp/profile/ja.jmTajpnU.html
出版者
出版者 JAPAN SOC ANALYTICAL CHEMISTRY
引用
内容記述タイプ Other
内容記述 BUNSEKI KAGAKU. 57(1): 61-65 (2008)
書誌情報 BUNSEKI KAGAKU

巻 57, 号 1, p. 61-65, 発行日 2008-01
資源タイプ(コンテンツの種類)
内容記述タイプ Other
内容記述 Article
ISSN
収録物識別子タイプ ISSN
収録物識別子 0525-1931
書誌レコードID
収録物識別子タイプ NCID
収録物識別子 AN00222633
DOI
識別子タイプ DOI
関連識別子 https://doi.org/10.2116/bunsekikagaku.57.61
関連名称 10.2116/bunsekikagaku.57.61
出版タイプ
出版タイプ AM
出版タイプResource http://purl.org/coar/version/c_ab4af688f83e57aa
WoS
表示名 Web of Science
URL http://gateway.isiknowledge.com/gateway/Gateway.cgi?&GWVersion=2&SrcAuth=ShinshuUniv&SrcApp=ShinshuUniv&DestLinkType=FullRecord&DestApp=WOS&KeyUT=000252607400009
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