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The M(2+)-doped alumina nanopowders (0-0.10 mass%) were prepared through a new sol-gel route using high-purity polyhydroxoaluminum (PHA) and MCl(2) solutions as starting materials. The composite gels obtained were calcined at 900 degrees C and ground by planetary ball milling. The powders were re-calcined at 900 degrees C to increase the content of a-alumina particles, which act as seeding for low-temperature densification. Densification and microstructural development depend on the M(2+) dopant species. Dense alumina ceramics (relative density \u003e= 99.0%) thus obtained had a uniform microstructure composed of fine grains, where the average grain size developed for non-doped, Ni-doped, Mg-doped and Ca-doped samples was 0.67, 0.67, 0.47 and 0.30 mu m, respectively, showing that Ca-doping is the most promising method for tailoring of nanocrystalline alumina ceramics. (c) 2008 Elsevier Ltd and Techna Group S.r.l. 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Fabrication of submicron alumina ceramics by pulse electric current sintering using M(2+) (M = Mg, Ca, Ni)-doped alumina nanopowders
http://hdl.handle.net/10091/13535
http://hdl.handle.net/10091/135353bd7ef4c-92d0-4b1a-ae5a-f4e0a54a12d3
名前 / ファイル | ライセンス | アクション |
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Item type | 学術雑誌論文 / Journal Article(1) | |||||
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公開日 | 2012-02-22 | |||||
タイトル | ||||||
言語 | en | |||||
タイトル | Fabrication of submicron alumina ceramics by pulse electric current sintering using M(2+) (M = Mg, Ca, Ni)-doped alumina nanopowders | |||||
言語 | ||||||
言語 | eng | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Sintering | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Sol-gel processes | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Grain size | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Al(2)O(3) | |||||
資源タイプ | ||||||
資源 | http://purl.org/coar/resource_type/c_6501 | |||||
タイプ | journal article | |||||
著者 |
Odaka, Atsushi
× Odaka, Atsushi× Yamaguchi, Tomohiro× Hida, Masahiro× Taruta, Seiichi× Kitajima, Kunio |
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信州大学研究者総覧へのリンク | ||||||
氏名 | Yamaguchi, Tomohiro | |||||
URL | http://soar-rd.shinshu-u.ac.jp/profile/ja.WVnVbpkh.html | |||||
信州大学研究者総覧へのリンク | ||||||
氏名 | Taruta, Seiichi | |||||
URL | http://soar-rd.shinshu-u.ac.jp/profile/ja.OacaZVkh.html | |||||
出版者 | ||||||
出版者 | ELSEVIER SCI LTD | |||||
引用 | ||||||
内容記述タイプ | Other | |||||
内容記述 | CERAMICS INTERNATIONAL. 35(5):1845-1850 (2009) | |||||
書誌情報 |
CERAMICS INTERNATIONAL 巻 35, 号 5, p. 1845-1850, 発行日 2009-07 |
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抄録 | ||||||
内容記述タイプ | Abstract | |||||
内容記述 | Dense submicron-grained alumina ceramics were fabricated by pulse electric current sintering (PECS) using M(2+)(M: Mg, Ca, Ni)-doped alumina nanopowders at 1250 degrees C under a uniaxial pressure of 80 MPa. The M(2+)-doped alumina nanopowders (0-0.10 mass%) were prepared through a new sol-gel route using high-purity polyhydroxoaluminum (PHA) and MCl(2) solutions as starting materials. The composite gels obtained were calcined at 900 degrees C and ground by planetary ball milling. The powders were re-calcined at 900 degrees C to increase the content of a-alumina particles, which act as seeding for low-temperature densification. Densification and microstructural development depend on the M(2+) dopant species. Dense alumina ceramics (relative density >= 99.0%) thus obtained had a uniform microstructure composed of fine grains, where the average grain size developed for non-doped, Ni-doped, Mg-doped and Ca-doped samples was 0.67, 0.67, 0.47 and 0.30 mu m, respectively, showing that Ca-doping is the most promising method for tailoring of nanocrystalline alumina ceramics. (c) 2008 Elsevier Ltd and Techna Group S.r.l. All rights reserved. | |||||
資源タイプ(コンテンツの種類) | ||||||
内容記述タイプ | Other | |||||
内容記述 | Article | |||||
ISSN | ||||||
収録物識別子タイプ | ISSN | |||||
収録物識別子 | 0272-8842 | |||||
書誌レコードID | ||||||
収録物識別子タイプ | NCID | |||||
収録物識別子 | AA10622625 | |||||
DOI | ||||||
識別子タイプ | DOI | |||||
関連識別子 | https://doi.org/10.1016/j.ceramint.2008.10.007 | |||||
関連名称 | 10.1016/j.ceramint.2008.10.007 | |||||
権利 | ||||||
権利情報 | Copyright© 2008 Elsevier Ltd and Techna Group S.r.l. | |||||
出版タイプ | ||||||
出版タイプ | AM | |||||
出版タイプResource | http://purl.org/coar/version/c_ab4af688f83e57aa | |||||
WoS | ||||||
表示名 | Web of Science | |||||
URL | http://gateway.isiknowledge.com/gateway/Gateway.cgi?&GWVersion=2&SrcAuth=ShinshuUniv&SrcApp=ShinshuUniv&DestLinkType=FullRecord&DestApp=WOS&KeyUT=000266524700017 |