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The effects of heat treatment on the coated VGCNFs were also studied. VGCNFs could be coated with a homogeneous Ni-B alloy film using a plating bath containing dimethylaminoborane (DMAB) as a reducing agent. The boron content of the Ni-B alloy film could be varied from 14 to 24 atom% B by varying the DMAB concentration of the plating bath. The VGCNFs were uniformly coated with a Ni-B alloy layer that was only several nanometers thick. The coating thickness on the VGCNFs could be controlled by varying the reaction time. The Ni-B alloy coatings formed in this study were semicrystalline or amorphous depending on the boron content of the alloy film. After heat treatment, the phase structure of the Ni-B alloy coatings changed to a stable crystalline structure consisting of a face-centered-cubic nickel phase and a Ni3B phase. 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The effects of heat treatment on the coated VGCNFs were also studied. VGCNFs could be coated with a homogeneous Ni-B alloy film using a plating bath containing dimethylaminoborane (DMAB) as a reducing agent. The boron content of the Ni-B alloy film could be varied from 14 to 24 atom% B by varying the DMAB concentration of the plating bath. The VGCNFs were uniformly coated with a Ni-B alloy layer that was only several nanometers thick. The coating thickness on the VGCNFs could be controlled by varying the reaction time. The Ni-B alloy coatings formed in this study were semicrystalline or amorphous depending on the boron content of the alloy film. After heat treatment, the phase structure of the Ni-B alloy coatings changed to a stable crystalline structure consisting of a face-centered-cubic nickel phase and a Ni3B phase. No cracks or exfoliation of the coatings were observed, even after heat treatment. (C) 2010 Elsevier Ltd. 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