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Gluconic acid and hydrazine were respectively used as the complexing and reducing agents for nickel ions. The deposits were heat-treated. The microstructures and magnetic properties of the deposits were examined. The MWCNTs were homogeneously coated with pure nickel and their surfaces were relatively bumpy. These pure-nickel-coated MWCNTs exhibited ferromagnetism and had higher magnetizations and coercivities than electroless Ni-P alloy-coated MWCNTs. The bumpy morphology of the pure-nickel coating became relatively smooth on heat-treatment. (C) 2010 The Electrochemical Society. 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