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In situ study of fiber structure development of poly(butylene terephthalate) in a continuous laser-heated drawing process
http://hdl.handle.net/10091/17801
http://hdl.handle.net/10091/178011e42d34b-0429-47f5-84fd-ec6d3689ee9c
| 名前 / ファイル | ライセンス | アクション |
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fiber_structure_development_poly_butylene_terephthalate.pdf (707.0 kB)
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| Item type | 学術雑誌論文 / Journal Article(1) | |||||||||||||||||||
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| 公開日 | 2014-08-06 | |||||||||||||||||||
| タイトル | ||||||||||||||||||||
| タイトル | In situ study of fiber structure development of poly(butylene terephthalate) in a continuous laser-heated drawing process | |||||||||||||||||||
| 言語 | ||||||||||||||||||||
| 言語 | eng | |||||||||||||||||||
| DOI | ||||||||||||||||||||
| 関連識別子 | https://doi.org/10.1038/pj.2012.65 | |||||||||||||||||||
| 関連名称 | 10.1038/pj.2012.65 | |||||||||||||||||||
| キーワード | ||||||||||||||||||||
| 主題 | crystal-crystal transition, laser-heated drawing, poly(butylene terephthalate) | |||||||||||||||||||
| 資源タイプ | ||||||||||||||||||||
| 資源 | http://purl.org/coar/resource_type/c_6501 | |||||||||||||||||||
| タイプ | journal article | |||||||||||||||||||
| 著者 |
Kim, Kyoung-Hou
× Kim, Kyoung-Hou
× Kang, Young-Ah
× Yokoyama, Aki
× Ikaga, Toshifumi
× Ohkoshi, Yutaka
× Wataoka, Isao
× Urakawa, Hiroshi
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| 信州大学研究者総覧へのリンク | ||||||||||||||||||||
| 氏名 | Kim, Kyoung-Hou | |||||||||||||||||||
| URL | http://soar-rd.shinshu-u.ac.jp/profile/ja.OpLajFkV.html | |||||||||||||||||||
| 信州大学研究者総覧へのリンク | ||||||||||||||||||||
| 氏名 | Ohkoshi, Yutaka | |||||||||||||||||||
| URL | http://soar-rd.shinshu-u.ac.jp/profile/ja.jUkejekV.html | |||||||||||||||||||
| 出版者 | ||||||||||||||||||||
| 出版者 | NATURE PUBLISHING GROUP | |||||||||||||||||||
| 引用 | ||||||||||||||||||||
| 内容記述 | POLYMER JOURNAL. 44(10):1030-1035 (2012) | |||||||||||||||||||
| 書誌情報 |
POLYMER JOURNAL 巻 44, 号 10, p. 1030-1035, 発行日 2012-10 |
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| 抄録 | ||||||||||||||||||||
| 内容記述 | The structural development of poly(butylene terephthalate) (PBT) fibers was analyzed using in situ wide angle X-ray diffraction and fiber temperature measurements during CO2 laser-heated drawing, in which the necking position on the running fiber could be fixed by CO2 laser irradiation. The measured parameters were determined as functions of the elapsed time after necking with a time resolution of 0.3 ms. The as-spun PBT fibers, which exhibited a low-oriented alpha-crystalline structure, were drawn to a draw ratio of 5 using laser heating. The (001') reflection, which indicates a quasi-smectic fibrillar structure, was not observed before crystallization in contrast to measurements of poly(ethylene terephthalate) (PET) and poly(ethylene 2,6-naphthalene dicarboxylate) (PEN). The alpha-crystal was transformed into an oriented beta-form crystal at the necking position, and the developed beta-crystallites exhibited increased size and altered orientation <2 ms after necking. The fiber temperature increased rapidly at around T-g, and the rearrangement of the beta-crystal primarily occurred as the fiber's temperature rose from 100 to 160 degrees C. The oriented beta-crystal of the drawn fiber transformed into the oriented beta-crystal when the drawing tension was released. Polymer Journal (2012) 44, 1030-1035; doi: 10.1038/pj.2012.65; published online 18 April 2012 | |||||||||||||||||||
| 資源タイプ（コンテンツの種類） | ||||||||||||||||||||
| ISSN | ||||||||||||||||||||
| 収録物識別子タイプ | ISSN | |||||||||||||||||||
| 収録物識別子 | 0032-3896 | |||||||||||||||||||
| 書誌レコードID | ||||||||||||||||||||
| 収録物識別子タイプ | NCID | |||||||||||||||||||
| 収録物識別子 | AA00777013 | |||||||||||||||||||
| 権利 | ||||||||||||||||||||
| 権利情報 | Copyright© 2013 The Society of Polymer Science, Japan | |||||||||||||||||||
| 出版タイプ | ||||||||||||||||||||
| 出版タイプ | AM | |||||||||||||||||||
| 出版タイプResource | http://purl.org/coar/version/c_ab4af688f83e57aa | |||||||||||||||||||
| WoS | ||||||||||||||||||||
| URL | http://gateway.isiknowledge.com/gateway/Gateway.cgi?&GWVersion=2&SrcAuth=ShinshuUniv&SrcApp=ShinshuUniv&DestLinkType=FullRecord&DestApp=WOS&KeyUT=000309672000006 | |||||||||||||||||||
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Kim, Kyoung-Hou, Kang, Young-Ah, Yokoyama, Aki, Ikaga, Toshifumi, Ohkoshi, Yutaka, Wataoka, Isao, Urakawa, Hiroshi, 2012, In situ study of fiber structure development of poly(butylene terephthalate) in a continuous laser-heated drawing process: NATURE PUBLISHING GROUP, 1030–1035 p.
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