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  1. 080 繊維学部
  2. 0801 学術論文

In situ study of fiber structure development of poly(butylene terephthalate) in a continuous laser-heated drawing process

http://hdl.handle.net/10091/17801
1e42d34b-0429-47f5-84fd-ec6d3689ee9c
名前 / ファイル ライセンス アクション
fiber_structure_development_poly_butylene_terephthalate.pdf fiber_structure_development_poly_butylene_terephthalate.pdf (707.0 kB)
Item type 学術雑誌論文 / Journal Article(1)
公開日 2014-08-06
タイトル
言語 en
タイトル In situ study of fiber structure development of poly(butylene terephthalate) in a continuous laser-heated drawing process
言語
言語 eng
キーワード
主題Scheme Other
主題 crystal-crystal transition
キーワード
主題Scheme Other
主題 laser-heated drawing
キーワード
主題Scheme Other
主題 poly(butylene terephthalate)
資源タイプ
資源 http://purl.org/coar/resource_type/c_6501
タイプ journal article
著者 Kim, Kyoung-Hou

× Kim, Kyoung-Hou

WEKO 40351

Kim, Kyoung-Hou

Search repository
Kang, Young-Ah

× Kang, Young-Ah

WEKO 40352

Kang, Young-Ah

Search repository
Yokoyama, Aki

× Yokoyama, Aki

WEKO 40353

Yokoyama, Aki

Search repository
Ikaga, Toshifumi

× Ikaga, Toshifumi

WEKO 40354

Ikaga, Toshifumi

Search repository
Ohkoshi, Yutaka

× Ohkoshi, Yutaka

WEKO 40355

Ohkoshi, Yutaka

Search repository
Wataoka, Isao

× Wataoka, Isao

WEKO 40356

Wataoka, Isao

Search repository
Urakawa, Hiroshi

× Urakawa, Hiroshi

WEKO 40357

Urakawa, Hiroshi

Search repository
信州大学研究者総覧へのリンク
氏名 Kim, Kyoung-Hou
URL http://soar-rd.shinshu-u.ac.jp/profile/ja.OpLajFkV.html
信州大学研究者総覧へのリンク
氏名 Ohkoshi, Yutaka
URL http://soar-rd.shinshu-u.ac.jp/profile/ja.jUkejekV.html
出版者
出版者 NATURE PUBLISHING GROUP
引用
内容記述タイプ Other
内容記述 POLYMER JOURNAL. 44(10):1030-1035 (2012)
書誌情報 POLYMER JOURNAL

巻 44, 号 10, p. 1030-1035, 発行日 2012-10
抄録
内容記述タイプ Abstract
内容記述 The structural development of poly(butylene terephthalate) (PBT) fibers was analyzed using in situ wide angle X-ray diffraction and fiber temperature measurements during CO2 laser-heated drawing, in which the necking position on the running fiber could be fixed by CO2 laser irradiation. The measured parameters were determined as functions of the elapsed time after necking with a time resolution of 0.3 ms. The as-spun PBT fibers, which exhibited a low-oriented alpha-crystalline structure, were drawn to a draw ratio of 5 using laser heating. The (001') reflection, which indicates a quasi-smectic fibrillar structure, was not observed before crystallization in contrast to measurements of poly(ethylene terephthalate) (PET) and poly(ethylene 2,6-naphthalene dicarboxylate) (PEN). The alpha-crystal was transformed into an oriented beta-form crystal at the necking position, and the developed beta-crystallites exhibited increased size and altered orientation <2 ms after necking. The fiber temperature increased rapidly at around T-g, and the rearrangement of the beta-crystal primarily occurred as the fiber's temperature rose from 100 to 160 degrees C. The oriented beta-crystal of the drawn fiber transformed into the oriented beta-crystal when the drawing tension was released. Polymer Journal (2012) 44, 1030-1035; doi: 10.1038/pj.2012.65; published online 18 April 2012
資源タイプ(コンテンツの種類)
内容記述タイプ Other
内容記述 Article
ISSN
収録物識別子タイプ ISSN
収録物識別子 0032-3896
書誌レコードID
収録物識別子タイプ NCID
収録物識別子 AA00777013
DOI
関連識別子
識別子タイプ DOI
関連識別子 https://doi.org/10.1038/pj.2012.65
関連名称
関連名称 10.1038/pj.2012.65
権利
権利情報 Copyright© 2013 The Society of Polymer Science, Japan
出版タイプ
出版タイプ AM
出版タイプResource http://purl.org/coar/version/c_ab4af688f83e57aa
WoS
表示名 Web of Science
URL http://gateway.isiknowledge.com/gateway/Gateway.cgi?&GWVersion=2&SrcAuth=ShinshuUniv&SrcApp=ShinshuUniv&DestLinkType=FullRecord&DestApp=WOS&KeyUT=000309672000006
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