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The in-situ WAXD/SAXS measurements were carried out with a high time-resolution of 0.4 ms. The as-spun iPP fibers of two different initial structures were laser-heat-drawn to a draw ratio of 6.5. For the drawing of PP fiber containing mesophase structure, diffraction from the oriented mesophase remained until an elapsed time of 1.0 ms, when oriented alpha-phase crystal started to form. Meanwhile, for the drawing of PP fiber containing both an alpha-phase and a mesophase structure, fragmented microcrystals were reorganized by orientation-induced crystallization before an elapsed time of 1.0 ms. The long period increased drastically with fragmentation, and decreased with reorganization. The long period was about 16 nm for both drawn fibers. (C) 2011 Elsevier Ltd. 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In-situ analysis of fiber structure development for isotactic polypropylene
http://hdl.handle.net/10091/16170
http://hdl.handle.net/10091/161706702c058-f523-4ca8-b5b7-bedfd9cc004f
名前 / ファイル | ライセンス | アクション |
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In-situ_analysis_fiber_structure_development_isotactic.pdf (444.3 kB)
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Item type | 学術雑誌論文 / Journal Article(1) | |||||
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公開日 | 2013-01-08 | |||||
タイトル | ||||||
言語 | en | |||||
タイトル | In-situ analysis of fiber structure development for isotactic polypropylene | |||||
言語 | ||||||
言語 | eng | |||||
DOI | ||||||
識別子タイプ | DOI | |||||
関連識別子 | https://doi.org/10.1016/j.polymer.2011.03.005 | |||||
関連名称 | 10.1016/j.polymer.2011.03.005 | |||||
キーワード | ||||||
主題 | Polypropylene, CO(2) laser drawing, Fiber structure development | |||||
資源タイプ | ||||||
資源 | http://purl.org/coar/resource_type/c_6501 | |||||
タイプ | journal article | |||||
著者 |
Kang, Young-Ah
× Kang, Young-Ah× Kim, Kyoung-Hou× Ikehata, Soichiro× Ohkoshi, Yutaka× Gotoh, Yasuo× Nagura, Masanobu× Urakawa, Hiroshi |
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信州大学研究者総覧へのリンク | ||||||
氏名 | Kim, Kyoung-Hou | |||||
URL | http://soar-rd.shinshu-u.ac.jp/profile/ja.OpLajFkV.html | |||||
信州大学研究者総覧へのリンク | ||||||
氏名 | Ohkoshi, Yutaka | |||||
URL | http://soar-rd.shinshu-u.ac.jp/profile/ja.jUkejekV.html | |||||
信州大学研究者総覧へのリンク | ||||||
氏名 | Gotoh, Yasuo | |||||
URL | http://soar-rd.shinshu-u.ac.jp/profile/ja.uVDmjekV.html | |||||
出版者 | ||||||
出版者 | ELSEVIER SCI LTD | |||||
引用 | ||||||
内容記述タイプ | Other | |||||
内容記述 | POLYMER. 52(9):2044-2050 (2011) | |||||
書誌情報 |
POLYMER 巻 52, 号 9, p. 2044-2050, 発行日 2011-04-19 |
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抄録 | ||||||
内容記述タイプ | Abstract | |||||
内容記述 | Structural development of isotactic polypropylene (iPP) fibers was analyzed in real time through in-situ WAXD/SAXS and fiber temperature measurements during CO(2) laser-heated drawing because the CO(2) laser irradiation can nearly fix the necking position on the running fiber. The in-situ WAXD/SAXS measurements were carried out with a high time-resolution of 0.4 ms. The as-spun iPP fibers of two different initial structures were laser-heat-drawn to a draw ratio of 6.5. For the drawing of PP fiber containing mesophase structure, diffraction from the oriented mesophase remained until an elapsed time of 1.0 ms, when oriented alpha-phase crystal started to form. Meanwhile, for the drawing of PP fiber containing both an alpha-phase and a mesophase structure, fragmented microcrystals were reorganized by orientation-induced crystallization before an elapsed time of 1.0 ms. The long period increased drastically with fragmentation, and decreased with reorganization. The long period was about 16 nm for both drawn fibers. | |||||
資源タイプ(コンテンツの種類) | ||||||
内容記述タイプ | Other | |||||
内容記述 | Article | |||||
ISSN | ||||||
収録物識別子タイプ | ISSN | |||||
収録物識別子 | 0032-3861 | |||||
書誌レコードID | ||||||
収録物識別子タイプ | NCID | |||||
収録物識別子 | AA00776983 | |||||
権利 | ||||||
権利情報 | Copyright© 2011 Elsevier Ltd. | |||||
出版タイプ | ||||||
出版タイプ | AM | |||||
出版タイプResource | http://purl.org/coar/version/c_ab4af688f83e57aa | |||||
WoS | ||||||
表示名 | Web of Science | |||||
URL | http://gateway.isiknowledge.com/gateway/Gateway.cgi?&GWVersion=2&SrcAuth=ShinshuUniv&SrcApp=ShinshuUniv&DestLinkType=FullRecord&DestApp=WOS&KeyUT=000289744400022 |