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Nylon 6, polypropylene, poly (ethylene terephthalate) and poly (L-lactide-co-\u03b5-caprolactone) fiber webs were prepared by the LES. For Nylon 6 and poly (L-lactide-co-\u03b5-caprolactone), fibers having average diameters of approximately 1 \u03bcm and a coefficient of variation (CV) of no more than 20% were obtained. The effects of the applied voltage and laser power on the diameter of the PET fibers were investigated. The average diameter of the electrospun PET fibers decreased with a decrease in the applied voltage; however, using an applied voltage that was too low caused thermodegradation. The average diameter decreased with an increase in laser power. 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Nylon 6, polypropylene, poly (ethylene terephthalate) and poly (L-lactide-co-epsilon-scaprolactone) fiber webs were prepared by the LES. For Nylon 6 and poly (L-lactide-co-epsilon-caprolactone), fibers having average diameters of approximately 1 mu m and a coefficient of variation (CV) of no more than 20% were obtained. The effects of the applied voltage and laser power on the diameter of the PET fibers were investigated. The average diameter of the electrospun PET fibers decreased with a decrease in the applied voltage; however, using an applied voltage that was too low caused thermodegradation. The average diameter decreased with an increase in laser power. 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