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  1. 080 繊維学部
  2. 0801 学術論文

Synthesis of Fluorescent Gelators and Direct Observation of Gelation with a Fluorescence Microscope

http://hdl.handle.net/10091/00021974
7efa18c8-8010-4b91-b7ab-75b0c443f89c
名前 / ファイル ライセンス アクション
15K05623_07.pdf 15K05623_07.pdf (1.7 MB)
Item type 学術雑誌論文 / Journal Article(1)
公開日 2020-03-12
タイトル
言語 en
タイトル Synthesis of Fluorescent Gelators and Direct Observation of Gelation with a Fluorescence Microscope
言語
言語 eng
キーワード
主題Scheme Other
主題 fluorescence
キーワード
主題Scheme Other
主題 fluorescence microscopy
キーワード
主題Scheme Other
主題 gels
キーワード
主題Scheme Other
主題 gelation
キーワード
主題Scheme Other
主題 gelators
資源タイプ
資源 http://purl.org/coar/resource_type/c_6501
タイプ journal article
著者 Hanabusa, Kenji

× Hanabusa, Kenji

WEKO 109169

Hanabusa, Kenji

Search repository
Ueda, Takuya

× Ueda, Takuya

WEKO 109170

Ueda, Takuya

Search repository
Takata, Shingo

× Takata, Shingo

WEKO 109171

Takata, Shingo

Search repository
Suzuki, Masahiro

× Suzuki, Masahiro

WEKO 109172

Suzuki, Masahiro

Search repository
信州大学研究者総覧へのリンク
氏名 Hanabusa, Kenji
URL http://soar-rd.shinshu-u.ac.jp/profile/ja.WCyNjekV.html
信州大学研究者総覧へのリンク
氏名 Suzuki, Masahiro
URL http://soar-rd.shinshu-u.ac.jp/profile/ja.WVnmjFkV.html
出版者
出版者 WILEY-V C H VERLAG GMBH
引用
内容記述タイプ Other
内容記述 CHEMISTRY-A EUROPEAN JOURNAL.22(47):16937-16947(2016)
書誌情報 CHEMISTRY-A EUROPEAN JOURNAL

巻 22, 号 47, p. 16937-16947, 発行日 2016-11-14
抄録
内容記述タイプ Abstract
内容記述 Fluorescein-, benzothiazole-, quinoline-, stilbene-, and carbazole-containing fluorescent gelators have been synthesized by connecting gelation-driving segments, including l-isoleucine, l-valine, l-phenylalanine, l-leucine residue, cyclo(l-asparaginyl-l-phenylalanyl), and trans-(1R,2R)-diaminocyclohexane. The emission behaviors of the gelators were investigated, and their gelation abilities studied against 15 solvents. The minimum gel concentration, variable-temperature spectroscopy, transmission electron microscopy, scanning electron microscopy, fluorescence microscopy (FM), and confocal laser scanning microscopy (CLSM) were used to characterize gelation. The intermolecular hydrogen bonding between the N-H and C=O of amide, van der Waals interactions and pi-pi stacking play important roles in gelation. The colors of emission are related to the fluorescence structures of gelators. Fibrous aggregates characterized by the color of their emission were observed by FM. 3D images are produced by the superposition of images captured by CLSM every 0.1 mu m to a settled depth. The 3D images show that the large micrometer-sized aggregates spread out three dimensionally. FM observations of mixed gelators are studied. In the case of gelation, two structurally related gelators with the same gelation-driving segment lead to the gelators build up of the same aggregates through similar hydrogen-bonding patterns. When two gelators with structurally different gelation-driving segments induce gelation, the gelators build up each aggregate through individual hydrogen-bonding patterns. A fluorescent reagent that was incorporated into the aggregates of gels through van der Waals interactions was developed. The addition of this fluorescent reagent enables the successful observation of nonfluorescent gelators' aggregates by FM.
資源タイプ(コンテンツの種類)
内容記述タイプ Other
内容記述 Article
ISSN
収録物識別子タイプ ISSN
収録物識別子 0947-6539
書誌レコードID
収録物識別子タイプ NCID
収録物識別子 AA11076269
PubMed
関連識別子
識別子タイプ PMID
関連識別子 https://www.ncbi.nlm.nih.gov/pubmed/27723140
関連名称
関連名称 27723140
DOI
関連識別子
識別子タイプ DOI
関連識別子 https://doi.org/10.1002/chem.201603295
関連名称
関連名称 10.1002/chem.201603295
権利
権利情報 This is the accepted version of the following article: Hanabusa K, Ueda T, Takata S, Suzuki M, Synthesis of Fluorescent Gelators and Direct Observation of Gelation with a Fluorescence Microscope, Chemistry—A European Journal , 10.1002/chem.201603295, 22, 47, (16937-16947), (2016), which has been published in final form at [https://doi.org/10.1002/chem.201603295]. This article may be used for non-commercial purposes in accordance with the Wiley Self-Archiving Policy [https://authorservices.wiley.com/authorresources/Journal-Authors/licensing/self-archiving.html].
出版タイプ
出版タイプ AM
出版タイプResource http://purl.org/coar/version/c_ab4af688f83e57aa
WoS
表示名 Web of Science
URL http://gateway.isiknowledge.com/gateway/Gateway.cgi?&GWVersion=2&SrcAuth=ShinshuUniv&SrcApp=ShinshuUniv&DestLinkType=FullRecord&DestApp=WOS&KeyUT=000387140200029
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