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  1. 080 繊維学部
  2. 0801 学術論文

First Total Synthesis of (+/-)-6 '-Methoxyretrojusticidin B Using Regiocontrolled Benzannulation: Structural Inconsistency with Procumphthalide A and Its Revision to 5 '-Methoxyretrochinensin

http://hdl.handle.net/10091/16152
ae08b09f-c363-403f-b12f-d73a0bbb68be
名前 / ファイル ライセンス アクション
First_Total_Synthesis_+-6-Methoxyretrojusticidin_B.pdf First_Total_Synthesis_+-6-Methoxyretrojusticidin_B.pdf (2.6 MB)
Item type 学術雑誌論文 / Journal Article(1)
公開日 2012-12-20
タイトル
言語 en
タイトル First Total Synthesis of (+/-)-6 '-Methoxyretrojusticidin B Using Regiocontrolled Benzannulation: Structural Inconsistency with Procumphthalide A and Its Revision to 5 '-Methoxyretrochinensin
言語
言語 eng
キーワード
主題Scheme Other
主題 total synthesis
キーワード
主題Scheme Other
主題 natural product
キーワード
主題Scheme Other
主題 annulation
キーワード
主題Scheme Other
主題 lignan lactone
キーワード
主題Scheme Other
主題 revised structure
資源タイプ
資源 http://purl.org/coar/resource_type/c_6501
タイプ journal article
著者 Yoshida, Eri

× Yoshida, Eri

WEKO 40782

Yoshida, Eri

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Yamashita, Daisuke

× Yamashita, Daisuke

WEKO 40783

Yamashita, Daisuke

Search repository
Sakai, Ryo

× Sakai, Ryo

WEKO 40784

Sakai, Ryo

Search repository
Tanabe, Yoo

× Tanabe, Yoo

WEKO 40785

Tanabe, Yoo

Search repository
Nishii, Yoshinori

× Nishii, Yoshinori

WEKO 40786

Nishii, Yoshinori

Search repository
信州大学研究者総覧へのリンク
氏名 Nishii, Yoshinori
URL http://soar-rd.shinshu-u.ac.jp/profile/ja.yeSUjFkV.html
出版者
出版者 GEORG THIEME VERLAG KG
引用
内容記述タイプ Other
内容記述 SYNLETT. 2010(15):2275-2278 (2010)
書誌情報 SYNLETT

巻 2010, 号 15, p. 2275-2278, 発行日 2010-09
抄録
内容記述タイプ Abstract
内容記述 We achieved the first total synthesis of a novel (+/-)-6'-methoxyretrojusticidin B, which was proposed as procumphthalide A, utilizing regiocontrolled benzannulation of an aryl(aryl')-2,2-dichlorocyclopropylmethanol as the key step. (1)H NMR spectral data suggested that the structure of the synthesized product, 6'-methoxyretrojusticidin B, was inconsistent with that of natural procumphthalide A. A computational study of the rotational barrier rationally supports the existence of a rigid chiral axis in 6'-methoxyretrojusticidin B. The revised structural elucidation of natural procumphthalide A was concluded to be 5'-methoxyretrochinensin.
資源タイプ(コンテンツの種類)
内容記述タイプ Other
内容記述 Article
ISSN
収録物識別子タイプ ISSN
収録物識別子 0936-5214
書誌レコードID
収録物識別子タイプ NCID
収録物識別子 AA10731110
DOI
関連識別子
識別子タイプ DOI
関連識別子 https://doi.org/10.1055/s-0030-1258529
関連名称
関連名称 10.1055/s-0030-1258529
権利
権利情報 Copyright© 2010 Georg Thieme Verlag Stuttgart
出版タイプ
出版タイプ AM
出版タイプResource http://purl.org/coar/version/c_ab4af688f83e57aa
WoS
表示名 Web of Science
URL http://gateway.isiknowledge.com/gateway/Gateway.cgi?&GWVersion=2&SrcAuth=ShinshuUniv&SrcApp=ShinshuUniv&DestLinkType=FullRecord&DestApp=WOS&KeyUT=000281516100010
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